Inorganic Chemicals Industry ›› 2021, Vol. 53 ›› Issue (12): 54-60.doi: 10.19964/j.issn.1006-4990.2021-0390
• Reviews and Special Topics • Previous Articles Next Articles
YUAN Biao(),WU Wei,LUO Chao,SHEN Peng,CHEN Zan
Received:
2021-07-21
Online:
2021-12-10
Published:
2021-12-16
CLC Number:
YUAN Biao,WU Wei,LUO Chao,SHEN Peng,CHEN Zan. Research progress on preparation and application of b-axis oriented MFI zeolite membranes[J]. Inorganic Chemicals Industry, 2021, 53(12): 54-60.
Table 1
Immersion and synthesis conditions of zeolite membranes[23]"
样品 | 特殊处理 | 合成 时间/h | 取向 | 完整性 | 厚度/ μm |
---|---|---|---|---|---|
S1 | — | 17 | b轴 | 不连续 | 8 |
S2 | 无TPAOH | 17 | 随机 | 不连续 | 9 |
S3 | 0.32 g TPAOH溶液浸渍 | 17 | a轴,b轴 | 连续 | 8 |
S4 | 0.08 g TPAOH溶液浸渍 | 17 | a轴,b轴 | 连续 | 8 |
S5 | — | 24 | 随机 | 连续 | 15 |
S6 | — | 5 | a轴 | 连续 | 3 |
S7 | 浸渍后真空处理 | 17 | 随机 | 连续 | 250 |
S8 | — | 17(旋转) | 随机 | 不连续 | 5 |
S9 | TPAOH溶液1∶3稀释, 垂直位置 | 17 | b轴 | 不连续 | 9 |
S10 | TPAOH溶液1∶3稀释,水平位置 | 17 | b轴 | 连续 | 10 |
S11 | TPAOH溶液1∶3稀释,垂直位置 | 48 | a轴,b轴 | 连续 | 8 |
S12 | TPAOH溶液1∶3稀释,水平位置 | 48 | a轴,b轴 | 连续 | 30 |
Fig.2
Schematic formation plot of TS-1 zeolite membranes on the glass modified by PVAc(a),SEM images of glass surface without PVAc treatment(b),TS-1 zeolite membranes on glasses treated with 1.73 g/m2 PVAc,19.07 g/m2 PVAc and 120.13 g/m2 PVAc(c,d,e);the inset in(d) is the corresponding cross section SEM image of (d)[25]"
Fig.3
Top(a~c) and side view(d~f) SEM images of b-oriented membranes:before(a,d) and after gel-free secondary growth for 6 h(b,e) and 12 h(c,f);enlarged TEM image showing the initial seed and newly grown sections and the irregular depths(g);growth mechanism(h);top and side (inset) view SEM images of a b-oriented membranes(i)[42]"
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