无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2012, Vol. 44 ›› Issue (11): 60-.

• 论文 • 上一篇    

蛋清作纳米反应器水热合成扇状纳米氧化锌

左白艳,李 领,孙 雨,高恩霜,宗 俊   

  1. 华东师范大学化学系,上海 200062
  • 出版日期:2012-11-10 发布日期:2012-11-09

Hydrothermal synthesis of fan-like nano-sized zinc oxide using egg albumin as a nanoreactor

 ZUO  Bai-Yan, LI  Ling, SUN  Yu, GAO  En-Shuang, ZONG  Jun   

  1. Department of Chemistry,East China Normal University,Shanghai 200062,China
  • Online:2012-11-10 Published:2012-11-09

摘要: 采用鸡蛋清作为纳米反应器,聚乙烯吡咯酮(PVP)作稳定剂,通过水热法合成了扇状纳米氧化锌。通过XRD、SEM、TEM、FT-IR、UV-Vis等分析方法对样品进行了表征,考察了样品对甲基橙溶液的光催化降解的性能,并初步讨论了这种扇形结构纳米氧化锌的形成机理。结果表明:该方法能简单、快速制备扇状纳米氧化锌材料,且得到的扇形样品具有很好的光催化性能。

关键词: 氧化锌, 纳米材料, 水热, 光催化

Abstract: Fan-like nano-sized zinc oxide were synthesized by hydrothermal process,using egg albumin as nanoreactor and polyvinylpyrrolidone(PVP) as stabilizer.The samples were characterized by X-ray diffraction(XRD),scanning electron microscope(SEM),transmission electron microscopy((TEM),Fourier transform infrared(FT-IR),and ultraviolet visual(UV-Vis) spectroscopy.The photocatalytic activity of the sample was also investigated by degradation of methyl orange. Furthermore,the formation mechanism of fan-like nano-sized zinc oxide was discussed in detail.Results showed that the method is a facile,effective way to synthesize fan-like nano-sized zinc oxide material and the obtained product has a good photocatalytic activity.

Key words: zinc oxide, nanomaterial, hydrothermal, photocatalysis

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