无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2012, Vol. 44 ›› Issue (1): 52-.

• 论文 • 上一篇    下一篇

酸浸渣综合回收浸铅工艺研究

 彭国敏, 俎小凤, 张福元   

  1. 河南中原黄金冶炼厂有限责任公司,河南三门峡 472000
  • 出版日期:2012-01-10 发布日期:2012-01-16

Study on leaching process of lead from acid residue

 PENG  Guo-Min, ZU  Xiao-Feng, ZHANG  Fu-Yuan   

  1. Henan Zhongyuan Gold Smelter Co.,Ltd.,Sanmenxia 472000,China
  • Published:2012-01-10 Online:2012-01-16

摘要: 针对氰化提金工艺酸浸渣中低品位金属铅的综合回收,采用盐浸法对金属铅进行了浸出实验研究,通过正交试验详细考察了浸出液固质量比、浸出温度、氯化钠浓度、浸出pH和浸出时间等因素对浸铅率的影响。结果表明,浸出液固质量比为5、浸出温度为333.15 K、氯化钠质量分数为30%、pH=0、浸出时间为4 h的实验条件下,最佳平均浸铅率为92.05%,相对标准偏差RSD=4.3‰;室温下最佳平均浸铅率为90.20%,RSD=4.1‰。因此,酸浸渣常温盐浸提铅是综合利用矿产资源回收铅及提高金、银回收率的有效途径。

关键词: 酸浸渣, 氯化钠, 浸出,

Abstract: In allusion to the comprehensive recovery of low-grade lead in acid residue from cyanidation process of golden leaching,salt leaching method was adopted to extract lead in the experimental study.Influences of the factors,such as liquid and solid (L/S) mass ratio,leaching temperature,leaching time,concentration of NaCl,and leaching pH,on leaching ratio of lead were studied through orthogonal experiment.It was found that when L/S mass ratio was 5,leaching tempeture was 333.15 K,mass fraction of NaCl was 30%,pH=0,and leaching time was 4 h the best average lead leaching rate was 92.05% and relatively standard deviation was 4.3‰.At room temperature,lead leaching rate also reached 90.20% and relatively standard deviation was 4.1‰.So salt leaching method is an effective way of lead recovery and gold and silver yield improvement in comprehensive utilization of mines at room temperature.

Key words: acid residue, NaCl, leaching, lead

中图分类号: