Inorganic Chemicals Industry ›› 2024, Vol. 56 ›› Issue (2): 95-103.doi: 10.19964/j.issn.1006-4990.2023-0197
• Environment·Health·Safety • Previous Articles Next Articles
ZHANG Li1(), ZHANG Dan2, PAN Hongyan1(), DONG Yonggang1(), LI Wenfei2, QIN Hong2
Received:
2023-04-06
Online:
2024-02-10
Published:
2024-02-06
Contact:
PAN Hongyan, DONG Yonggang
E-mail:3431183060@qq.com;cepanhongyan@163.com;ygdong@gzu.edu.cn
CLC Number:
ZHANG Li, ZHANG Dan, PAN Hongyan, DONG Yonggang, LI Wenfei, QIN Hong. Study on preparation of low ash activated carbon by phosphoric acid method[J]. Inorganic Chemicals Industry, 2024, 56(2): 95-103.
Table 1
Pore structure parameters of activated carbon prepared at different activation temperatures"
样品 | SBET/ (m2·g-1) | Smic/ (m2·g-1) | Smes/ (m2·g-1) | Vtotal/ (cm3·g-1) | Vmic/ (cm3·g-1) | Vmes/ (cm3·g-1) |
---|---|---|---|---|---|---|
AC-450 | 1 677 | 1 330 | 347 | 1.056 9 | 0.686 6 | 0.370 3 |
AC-500 | 1 762 | 1 406 | 356 | 1.065 8 | 0.690 4 | 0.375 4 |
AC-550 | 2 103 | 1 818 | 285 | 1.151 3 | 0.869 9 | 0.272 3 |
Table 3
Pore structure parameters of activated carbon prepared at different phosphoric acid concentrations"
样品 | SBET/ (m2·g-1) | Smic/ (m2·g-1) | Smes/ (m2·g-1) | Vtotal/ (cm3·g-1) | Vmic/ (cm3·g-1) | Vmes/ (cm3·g-1) |
---|---|---|---|---|---|---|
AC-56 | 1 762 | 1 406 | 356 | 1.065 8 | 0.690 4 | 0.375 4 |
AC-70 | 2 290 | 1 690 | 600 | 1.501 8 | 0.849 6 | 0.652 2 |
AC-85 | 1 787 | 1 329 | 458 | 1.199 2 | 0.759 1 | 0.440 1 |
Table 4
Pore structure parameters of activated carbon prepared at different acid chip mass ratios"
样品 | SBET/ (m2·g-1) | Smic/ (m2·g-1) | Smes/ (m2·g-1) | Vtotal/ (cm3·g-1) | Vmic/ (cm3·g-1) | Vmes/ (cm3·g-1) |
---|---|---|---|---|---|---|
AC-1.5 | 1 522 | 1 314 | 208 | 0.90 | 0.70 | 0.20 |
AC-2.0 | 1 762 | 1 406 | 356 | 1.07 | 0.69 | 0.38 |
AC-2.5 | 1 831 | 1 573 | 258 | 1.12 | 0.85 | 0.27 |
AC-3.5 | 1 547 | 401 | 1 146 | 1.44 | 0.26 | 1.18 |
1 | 邓美玲.关于活性炭市场调研的建模分析[J].科技与创新,2022(20):109-111. |
DENG Meiling.Modeling and analysis of activated carbon market research[J].Science and Technology & Innovation,2022(20):109-111. | |
2 | 任学勇,祁项超,曹畅,等.“双碳”战略下生物质活性炭材料生产与应用发展探析[J].林产工业,2022,59(4):48-51,63. |
REN Xueyong, QI Xiangchao, CAO Chang,et al.Research on production and application of biomass activated carbon under “double carbon” strategy[J].China Forest Products Industry,2022,59(4):48-51,63. | |
3 | 孙昊,孙云娟,缪存标,等.我国活性炭产业发展典型案例分析:以福建元力活性炭股份有限公司为例[J].生物质化学工程,2021,55(1):1-9. |
SUN Hao, SUN Yunjuan, MIAO Cunbiao,et al.A typical case analysis of activated carbon industry development in China:Fujian Yuanli active carbon Co.,Ltd.[J].Biomass Chemical Engineering,2021,55(1):1-9. | |
4 | 解强,张香兰,梁鼎成,等.煤基活性炭定向制备:原理·方法·应用[J].煤炭科学技术,2021,49(1):100-127. |
XIE Qiang, ZHANG Xianglan, LIANG Dingcheng,et al.Directional preparation of coal-based activated carbon:Principles,approaches and applications[J].Coal Science and Technology,2021,49(1):100-127. | |
5 | 王硕,张健本,谢彩锋.生物质活性炭制备及吸附含硫化合物研究进展[J].应用化工,2022,51(12):3608-3613. |
WANG Shuo, ZHANG Jianben, XIE Caifeng.Preparation and adsorption of sulfur compounds by biomass activated carbon[J].Applied Chemical Industry,2022,51(12):3608-3613. | |
6 | TRIFONOV S V, MURYGIN A V, TIKHOMIROV A A.Physical-chemical method for desalting organic waste for agricultural cycl-es[J].IOP Conference Series:Earth and Environmental Science,2021,839(4):042062. |
7 | 张会均,欧阳晚秋,陈琳莉.磷酸法茶渣活性炭的制备及吸附性能[J].应用化工,2019,48(12):2947-2950. |
ZHANG Huijun, OUYANG Wanqiu, CHEN Linli.Characteristics and optimization of activated carbon from tea waste using H3PO4 [J].Applied Chemical Industry,2019,48(12):2947-2950. | |
8 | 郭奇,许伟,刘军利.磷酸法木质素基活性炭的制备及其电化学性能研究[J].林产化学与工业,2022,42(2):31-38. |
GUO Qi, XU Wei, LIU Junli.Preparation and electrochemical performance of lignin-based activated carbon by phosphoric acid activation[J].Chemistry and Industry of Forest Products,2022,42(2):31-38. | |
9 | KAMAL S, AHMED B.Experimental tests of cadmium and trace metals adsorption on natural clays and activated carbon from wet phosphoric acid[J].Inorganic Chemistry Communications,2022,144:109866. |
10 | MUNAWAR I, MUHAMMAD S, ZAHID A,et al.Paracetamol and amoxicillin adsorptive removal from aqueous solution using phosphoric acid activated-carbon[J].Zeitschrift Für Physikalische Chemie,2023,237(3):257-271. |
11 | HIGAI D, HUANG Zhebin, QIAN E W.Preparation and surface characteristics of phosphoric acid-activated carbon from coconut shell in air[J].Environmental Progress & Sustainable Energy,2021,40(2):e13509. |
12 | 李文飞,王凤霞,杨坤.湿法净化磷酸与热法磷酸在微生物发酵应用中的差异研究[J].广州化工,2021,49(3):46-49. |
LI Wenfei, WANG Fengxia, YANG Kun.Study on difference between purified wet phosphoric acid and thermal method phosphoric acid in microbial fermentation[J].Guangzhou Chemical Industry,2021,49(3):46-49. | |
13 | 马航,冯霄.基于湿、热法磷加工体系共生耦合的磷资源产业可持续性发展研究[J].无机盐工业,2018,50(11):1-6. |
MA Hang, FENG Xiao.Study on sustainable development of phosphorus industry based on symbiotic coupling of wet and thermal phosphorus processing systems[J].Inorganic Chemicals Industry,2018,50(11):1-6. | |
14 | 梅毅,樊蕾,梁雪松,等.热法磷酸与湿法工业磷酸的技术经济分析[J].无机盐工业,2011,43(1):4-7. |
MEI Yi, FAN Lei, LIANG Xuesong,et al.Techno-economic analysis on phosphoric acid by furnace process and phosphoric acid by wet process[J].Inorganic Chemicals Industry,2011,43(1):4-7. | |
15 | 王保明,吕中豪,李会勇,等.湿法磷酸制备磷酸脲的研究进展[J].无机盐工业,2020,52(11):1-5. |
WANG Baoming, Zhonghao LÜ, LI Huiyong,et al.Research progress on preparation of urea phosphate with wet-process phosphoric acid[J].Inorganic Chemicals Industry,2020,52(11):1-5. | |
16 | 杜加磊,翟持,朱远蹠,等.基于分析的热法磷酸全热能回收技术模拟研究[J].化工学报,2021,72(11):5790-5799. |
DU Jialei, ZHAI Chi, ZHU Yuanzhi,et al.Simulation study on heat energy recovery technology of furnace-process phosphoric acid process[J].CIESC Journal,2021,72(11):5790-5799. | |
17 | 齐亚兵,张思敬.湿法磷酸净化技术研究新进展及应用现状[J].应用化工,2022,51(9):2798-2804. |
QI Yabing, ZHANG Sijing.New research progress and present application situation of purification technology for wet-process phosphoric acid[J].Applied Chemical Industry,2022,51(9):2798-2804. | |
18 | 王芳平,张劲斌,李晨阳,等.灰分对玉米芯基活性炭电化学性能的影响[J].现代化工,2020,40(5):190-193. |
WANG Fangping, ZHANG Jinbin, LI Chenyang,et al.Effect of ash on electrochemical performance of corncob-based activated carbon[J].Modern Chemical Industry,2020,40(5):190-193. | |
19 | 刘菲.酸洗除灰分对活性炭性质的影响[J].石化技术,2019,26(5):212-213. |
LIU Fei.Effect of acid cleaning and ash removal on properties of activated carbon[J].Petrochemical Industry Technology,2019,26(5):212-213. | |
20 | 邵远超,田华宇,王国睿,等.低灰分刺竹炭制备及性能表征[J].林业工程学报,2023,8(1):80-87. |
SHAO Yuanchao, TIAN Huayu, WANG Guorui,et al.Study on preparation and characterization of low ash bambusa sinospinosa charcoal[J].Journal of Forestry Engineering,2023,8(1):80-87. | |
21 | 鲍建秀.磷酸法制备低灰分活性炭的研究[J].化学工程与装备,2019(4):19-20,42. |
BAO Jianxiu.Study on preparation of low ash activated carbon by phosphoric acid method[J].Chemical Engineering & Equipment,2019(4):19-20,42. | |
22 | 徐茹婷,卢辛成,许伟,等.磷酸法玉米秸秆基活性炭的制备及其表征[J].生物质化学工程,2022,56(1):1-6. |
XU Ruting, LU Xincheng, XU Wei,et al.Preparation and characterization of corn straw based activated carbon by phosphoric acid activation[J].Biomass Chemical Engineering,2022,56(1):1-6. | |
23 | 叶结旺,周志丹,金贞福.氮掺杂木质素基活性炭的制备、表征及其吸附性能研究[J].林产化学与工业,2023,43(1):127-132. |
YE Jiewang, ZHOU Zhidan, JIN Zhenfu.Preparation,characterization and adsorption properties of nitrogen-doped lignin-based activated carbon[J].Chemistry and Industry of Forest Products,2023,43(1):127-132. | |
24 | 马名哲,孙昊,孙康,等.龙凤檀磷酸法活性炭的孔径分布与吸附性能的构效关系[J].林产化学与工业,2023,43(1):51-56. |
MA Mingzhe, SUN Hao, SUN Kang,et al.The relationship between pore size distribution and adsorption properties of cumaru activated carbon prepared by phosphoric acid method[J].Chemistry and Industry of Forest Products,2023,43(1):51-56. | |
25 | MAGUANA Y EL, ELHADIRI N, BOUCHDOUG M,et al.Activated carbon from prickly pear seed cake:Optimization of preparation conditions using experimental design and its application in dye removal[J].International Journal of Chemical Engineering,2019,2019(12):1-12. |
26 | DENG Meigen, WANG Junlong, ZHANG Qi.Effect of freezing pretreatment on the performance of activated carbon from coconut shell for supercapacitor application[J].Materials Letters,2022,306:130934. |
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