Inorganic Chemicals Industry ›› 2022, Vol. 54 ›› Issue (9): 96-101.doi: 10.19964/j.issn.1006-4990.2021-0741
• Research & Development • Previous Articles Next Articles
DU Bingxuan(),LI Haichao(),LIN Zezhong
Received:
2021-11-23
Online:
2022-09-10
Published:
2022-09-22
Contact:
LI Haichao
E-mail:tangchaolizi_225@sina.com;lihaichao@vip.163.com
CLC Number:
DU Bingxuan,LI Haichao,LIN Zezhong. Study on preparation of food?grade potassium chloride by one?step adsorption and purification[J]. Inorganic Chemicals Industry, 2022, 54(9): 96-101.
Table 3
Contents of various substances duringadsorption of industrial potassium chloride"
鱼鳞活性炭投加量/(g·L) | w(氯化 钾)/% | 杂质含量/(mg·kg-1) | ||||
---|---|---|---|---|---|---|
钙 | 镁 | 铅 | 十八胺 | 砷 | ||
0 | 95.131 | 46.300 | 30.100 | 16.300 | 169.800 | 未检出 |
1 | 97.384 | 未检出 | 未检出 | 10.240 | 115.890 | 未检出 |
2 | 未检测 | 未检出 | 未检出 | 3.239 | 70.404 | 未检出 |
3 | 98.760 | 未检出 | 未检出 | 1.254 | 37.276 | 未检出 |
4 | 未检测 | 未检出 | 未检出 | 0.941 | 17.058 | 未检出 |
5 | 99.139 | 未检出 | 未检出 | 0.766 | 13.694 | 未检出 |
7 | 99.259 | 未检出 | 未检出 | 未检出 | 未检出 | 未检出 |
9 | 99.339 | 未检出 | 未检出 | 未检出 | 未检出 | 未检出 |
[1] | 李兴海,赵启文,李秦鹏,等.利用低品位钾资源制备钾石盐实验研究[J].无机盐工业,2018,50(7):51-53. |
LI Xinghai, ZHAO Qiwen, LI Qinpeng, et al.Experimental study on preparation of sylvite from low⁃grade potassium resources[J].Inorganic Chemicals Industry,2018,50(7):51-53. | |
[2] | 刁祥瑞,张洪满,张君,等.分光光度法测定氯化钾浮选液中十八胺含量[J].中北大学学报:自然科学版,2011,32(3):323-328. |
DIAO Xiangrui, ZHANG Hongman, ZHANG Jun, et al.Spectrophotometric determination of octadecylamine in brine from KCl flotation[J].Journal of North University of China:Natural Science Edition,2011,32(3):323-328. | |
[3] | 费文丽,李贵林.大孔树脂吸附法处理卤水中钾盐浮选捕收剂十八胺[J].化工矿物与加工,2012,41(4):17-20. |
FEI Wenli, LI Guilin.Treatment of sylvite flotation collector octadecylamine in brine with macroporous resin adsorption method[J].Industrial Minerals & Processing,2012,41(4):17-20. | |
[4] |
LIU Runqing, LU Hongyu, WANG Li, et al.Utilization of ammonium chloride as a novel selective depressant in reverse flotation of potassium chloride[J].Minerals,2019,9(1).Doi:10.3390/min9010041.
doi: 10.3390/min9010041. |
[5] | 梁慧斌,杜志平,李恩泽,等.金橙-2分光光度法测定饱和盐溶液中十八胺盐酸盐的含量[J].日用化学工业,2016,46(8):485-488. |
LIANG Huibin, DU Zhiping, LI Enze, et al.Determination of octadecylamine hydrochloride in saturated salt solution using orange Ⅱ spectrophotometric method[J].China Surfactant Detergent & Cosmetics,2016,46(8):485-488. | |
[6] | 王宝辉,张学佳,纪巍,等.表面活性剂环境危害性分析[J].化工进展,2007,26(9):1263-1268. |
WANG Baohui, ZHANG Xuejia, JI Wei, et al.Hazard analysis of surfactants in ecosystem[J].Chemical Industry and Engineering Progress,2007,26(9):1263-1268. | |
[7] |
EMAMY F H, BUMAJDAD A, LUKASZEWICZ J P.Adsorption of hexavalent chromium and divalent lead ions on the nitrogen⁃enriched chitosan⁃based activated carbon[J].Nanomaterials:Basel,Switzerland,2021,11(8).Doi:10.3390/nano11081907.
doi: 10.3390/nano11081907. |
[8] | 李明达.一种除去氯化钾中铵的方法:中国,104192866A[P].2014-12-10. |
[9] | 许超锋,王国平,汪贤玉,等.低钠高纯度氯化钾的生产方法:中国,105668592A[P].2016-06-15. |
[10] | 刘立平,马信华,王朝乾.精制氯化钾生产工艺:中国,101962198A[P].2011-02-02. |
[11] | 柯曾鹏,杨帅敏,杨志国,等.采用吸附工艺生产食品级氯化钾的方法:中国,105060315A[P].2015-11-18. |
[12] | 钟林,钟国林,韩科.食品级氯化钾的制造工艺方法中国,103833052A[P].2014-06-04. |
[13] | 熊新国,王虎臣,刘宗飞,等.一种高纯食品级氯化钾的生产方法:中国,106495189A[P].2017-03-15. |
[14] | 孙书双,朱亚明,赵先奕,等.生物质活性炭的制备、应用及再生利用研究进展[J].应用化工,2021,50(11):3165-3170. |
SUN Shushuang, ZHU Yaming, ZHAO Xianyi, et al.Research progress on preparation,application and regeneration of biomass⁃based activated carbon[J].Applied Chemical Industry,2021,50(11):3165-3170. | |
[15] | 张净净,李海朝.磷酸活化鱼鳞活性生物炭的制备及表征[J].材料导报,2020,34(S1):116-119. |
ZHANG Jingjing, LI Haichao.Preparation and characterization of fish scale activated carbon by phosphoric acid[J].Materials Reports,2020,34(S1):116-119. | |
[16] | PATI F, ADHIKARI B, DHARA S.Isolation and characterization of fish scale collagen of higher thermal stability[J].Bioresource Technology,2010,101(10):3737-3742. |
[17] |
QIN Di, BI Shichao, YOU Xinguo, et al.Development and application of fish scale wastes as versatile natural biomaterials[J].Chemical Engineering Journal,2022,428.Doi:10.1016/j.cej.2021.131102.
doi: 10.1016/j.cej.2021.131102. |
[18] | 李海朝,纪青松,张净净,等.活性生物猪骨炭纯化盐湖工业氯化钾[J].无机盐工业,2020,52(8):76-77,102. |
LI Haichao, JI Qingsong, ZHANG Jingjing, et al.Purification of industrial potassium chloride from salt lake by activated pig bone biochar[J].Inorganic Chemicals Industry,2020,52(8):76-77,102. | |
[19] | 徐茹婷,许伟,卢辛成,等.磷酸法木质活性炭除灰新工艺研究[J].生物质化学工程,2020,54(4):37-41. |
XU Ruting, XU Wei, LU Xincheng, et al.Novel demineralization technology of phosphate⁃activated carbon[J].Biomass Chemical Engineering,2020,54(4):37-41. | |
[20] | NADEEM R, ANSARI T M, KHALID A M.Fourier Transform Infrared Spectroscopic characterization and optimization of Pb(Ⅱ) biosorption by fish(Labeo rohita) scales[J].Journal of Hazardous Materials,2008,156(1/2/3):64-73. |
[21] | KAPOOR A, VIRARAGHAVAN T.Biosorption of heavy metals on Aspergillus Niger:Effect of pretreatment[J].Bioresource Tech⁃ nology,1998,63(2):109-113. |
[22] | FERREIRA L M, MELO R R, PIMENTA A S, et al.Adsorption performance of activated charcoal from castor seed cake prepared by chemical activation with phosphoric acid[J].Biomass Conversion and Biorefinery,2022,12(4):1181-1192. |
[23] | ONWORDI C T, UCHE C C, AMEH A E, et al.Comparative study of the adsorption capacity of lead(Ⅱ) ions onto bean husk and fish scale from aqueous solution[J].Journal of Water Reuse and Desalination,2019,9(3):249-262. |
[24] | VILLANUEVA-ESPINOSA J F, HERNÁNDEZ-ESPARZA M, RUIZ-TREVIÑO F A.Adsorptive properties of fish scales of oreochromis niloticus(mojarra tilapia) for metallic ion removal from waste water[J].Industrial & Engineering Chemistry Research,2001,40(16):3563-3569. |
[25] | EL-NAGAR D A, MASSOUD S A, ISMAIL S H.Removal of some heavy metals and fungicides from aqueous solutions using nano⁃hydroxyapatite,nano⁃bentonite and nanocomposite[J].Arabian Journal of Chemistry,2020,13(11):7695-7706. |
[26] | 梁志,车文成,胡鑫鑫.罗非鱼鱼鳞对水中结晶紫的吸附特性和机理研究[J].化工新型材料,2019,47(4):208-212. |
LIANG Zhi, CHE Wencheng, HU Xinxin.Adsorption of crystal violet dye on fish(tilapia) scale:Characteristics and mechanism[J].New Chemical Materials,2019,47(4):208-212. | |
[27] | SHAARANI F W, HAMEED B H.Ammonia⁃modified activated carbon for the adsorption of 2,4-dichlorophenol[J].Chemical Engineering Journal,2011,169(1/2/3):180-185. |
[28] | QU Zhibin, SUN Fei, LIU Xin, et al.The effect of nitrogen⁃containing functional groups on SO2 adsorption on carbon surface:Enhanced physical adsorption interactions[J].Surface Science,2018,677:78-82. |
[29] | WANG Gaofeng, XU Jie, SUN Zhiming, et al.Surface functionalization of montmorillonite with chitosan and the role of surface properties on its adsorptive performance:A comparative study on mycotoxins adsorption[J].Langmuir:the ACS Journal of Surfaces and Colloids,2020,36(10):2601-2611. |
[30] | YANG Guo, CHEN Honglin, QIN Hangdao, et al.Amination of activated carbon for enhancing phenol adsorption:Effect of nitro⁃gen⁃containing functional groups[J].Applied Surface Science,2014,293:299-305. |
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