无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2016, Vol. 48 ›› Issue (7): 48-.

• 论文 • 上一篇    下一篇

分析纯元明粉生产新工艺

张淑样   

  1. 南风集团技术中心,山西运城 044000
  • 出版日期:2016-07-10 发布日期:2016-07-25

Novel production process of analytical grade sodium sulfate

 ZHANG  Shu-Yang   

  1. Technique Center,Nafine Chemical Group,Yuncheng 044000,China
  • Published:2016-07-10 Online:2016-07-25

摘要: 详细地阐述了以元明粉生产过程中的半成品(即离心机分离的湿元明粉)90硝为原料,经过溶解、除钙镁、调pH、蒸发、分离、干燥等一系列工序,生产出符合《化学试剂无水硫酸钠》GB/T 9853—2008技术指标的分析纯元明粉。主要中控参数:溶液pH为3~6,蒸发终点控制在母液中Ca2+质量浓度≤0.55 g/L。该工艺生产分析纯元明粉,具有工艺过程简单,产品溶解性好、纯度高、质量稳定,辅料廉价易得,生产成本小、利润空间大等优点,值得在高纯元明粉行业推广应用。

关键词: 分析纯元明粉, 控制pH, 硫酸钠

Abstract: The production of analytical grade sodium sulfate,which matches GB/T 9853—2008,by using 90% sodium sulfate(the semi-finished wet products collected from centrifuge) obtained from the general process as raw material has been presented.The procedures generally include dissolution,pH adjusting,evaporation,separation,and drying etc..The main central parameters are that the solution pH must be between 3~6,and the terminal control point in evaporation requires that the concentration of Ca2+ ions within the mother liquor must be no more than 0.55 g/L.It is assumed that the as-prepared analytical grade sodium sulfate products are of high solubility,high purity,and stable quality.Moreover,the process is also of great advantages of simple,low cost,and high profit,which promise it expansive potentials.

Key words: analytical grade sodium sulfate, pH controlling, sodium sulfate

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