无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2015, Vol. 47 ›› Issue (6): 60-.

• 论文 • 上一篇    下一篇

新型吸附材料制备及处理含DMAC废水试验研究*

伏广龙1,2,张雁秋1,祝春水2   

  1. 1.中国矿业大学环境与测绘工程学院,江苏徐州 221116;2.淮海工学院化学工程学院
  • 出版日期:2015-06-10 发布日期:2015-05-22

 Preparation of a new type of adsorption material to treat DMAC contained wastewater 

Fu Guanglong1,2,Zhang Yanqiu1,Zhu Chunshui2   

  1. 1.School of Environment Science and Spatial Informatics,China University of Mining & Technology,Xuzhou 221116,China;
    2.School of Chemical Engineering; Huaihai Institute of Technology
  • Online:2015-06-10 Published:2015-05-22

摘要: 合成了主要成分为粉煤灰和活性炭的新型吸附材料,并通过单因素试验考察了吸附材料处理含DMAC(N, N-二甲基乙酰胺)废水的效果。吸附材料最佳制备条件:粉煤灰与活性炭质量比为3∶1,硅酸钠加入量为25%(硅酸钠占粉煤灰、活性炭、硅酸钠总质量的质量分数),煅烧温度为800 ℃。吸附材料处理含N, N-二甲基乙酰胺废水最佳条件:pH为3,吸附剂投加量为25 g/L,吸附时间为40 min,吸附温度为30 ℃,在此条件下CODCr去除率为75.92 %。

关键词: 粉煤灰, 硅酸钠, N, N-二甲基乙酰胺, 活性炭

Abstract: The adsorption performance of a new type of adsorption material based on the fly ash and activated carbon as main contents was researched.The effect of it treating DMAC(N,N-dimethyl acetamide) contained wastewater was investigated by the single factor experiment.The optimum preparation conditions:the mass ratio of fly ash to activated carbon was 3∶1,sodium silicate dosage was 25%(mass fraction of sodium silicate accounts for total mass of fly ash,activated carbon,and sodium silicate), and the calcining temperature was 800 ℃.The optimum conditions of the new material treating the DMAC wastewater were: pH was 3,adsorbent dosage was 25 g/L,absorbing time was 40 min,and absorbing temperature was 30 ℃.The removal rate of CODCr reached 75.92% under the best conditions.

Key words: fly ash, sodium silicate, DMAC, activated carbon