INORGANICCHEMICALSINDUSTRY ›› 2013, Vol. 45 ›› Issue (2): 45-.

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Research on separation and recycling of waste mortar produced in solar silicon cutting

YANG  Rong-Hua, ZHAO  Chuan-Hua, ZHANG  Chun-Xue, DU  Jin-Feng, CHENG  Pan-Xia   

  1. School of Chemical Engineering,Taishan Medical University,Taian 271016,China
  • Online:2013-02-10 Published:2013-02-21

Abstract: Impurities of iron and stainless steel powder etc. in the waste mortar produced in solar silicon cutting were removed and polyethylene glycol(PEG),silicon,and silicon carbide were recovered by liquid-solid separation,acid-dissolve,and alkali-dissolve depuration methods.Results indicated,using water as solvent,with liquid volume to solid mass ratio(mL/g) of 10∶1, stirring time of 10 min at room temperature,PEG in waste mortar could be dissolved and it could be recovered by the following distillation method;the optimal process conditions of removing iron and stainless steel powder with hydrochloric acid were: c(HCl)=3.0 mol/L, temperature was 40 ℃,reaction time was 1 h,and liquid/solid ratio was 10∶1;using acid-dissolve and alkali-dissolve methods to remove silicon,could make the mass fraction of silicon in silicon carbide powder drop to 0.5% below.

Key words: waster mortar, silicon carbide, silicon, polyethylene glycol

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