Inorganic Chemicals Industry ›› 2020, Vol. 52 ›› Issue (9): 26-31.doi: 10.11962/1006-4990.2019-0523

• Research & Development • Previous Articles     Next Articles

Preparation of PS/Ag-SiO2-Au organic-inorganic bimetallic hybrid particles

Mei Shuxing1,2(),Pang Shuanlin2,Pan Mingwang1(),Xie Zhiyong2,Li Zhishui2   

  1. 1. Institute of Chemical Engineering and Technology,Hebei University of Technology,Tianjin 300130,China
    2. Tianjin Bohua Yongli Chemical Co.,Ltd.
  • Received:2020-03-14 Online:2020-09-10 Published:2020-09-27
  • Contact: Pan Mingwang E-mail:meishuxingtjuci@163.com;mwpan@126.com

Abstract:

PS/SiO2-Au organic-inorganic hybrid particles were obtained by reacting organic polystyrene dimer(PsD) with inorganic SiO2-Au particles.The snowman-shape of PsD particles and SiO2-Au particles were obtained via seed emulsion polymerization and sol-gel method,respectively.On the basis of PS/SiO2-Au particles,nano-sized Ag particles were supported on it to obtain bimetallic hybrid particles PS/Ag-SiO2-Au.During the period,effects of the ratios between monomers and polymer seeds,the adding amount of ammonia on morphology of the organic and inorganic particles were discussed.Infrared(FT-IR),scanning electron microscopy(SEM),energy spectrum analysis(EDS),transmission electron microscopy(TEM)and laser particle size tester(DLS) were used to characterize the structure,morphology,composition and size of the obtained particles.The prepared PS/Ag-SiO2-Au hybrid particles will have potential applications in the field of catalysis.

Key words: polystyrene dimers, silica, hybrid particles

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