无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2014, Vol. 46 ›› Issue (10): 39-.

• 论文 • 上一篇    下一篇

碳酸盐型盐湖提取钾芒硝浮选工艺研究

胡兆军1,2,张志宏2,董生发2,马艳芳2,付振海2,安 东1,2   

  1. 1.中国科学院大学,北京 100049;2.中国科学院青海盐湖研究所
  • 出版日期:2014-10-10 发布日期:2014-10-09

Research on technology of processing glaserite from carbonate-based salt lake by flotation method

Hu Zhaojun1,2,Zhang Zhihong2,Dong Shengfa2,Ma Yanfang2,Fu Zhenhai2,An Dong1,2   

  1. 1.University of Chinese Academy of Sciences,Beijing 100049,China;
    2.Qinghai Institute of Salt Lakes,Chinese Academy of Sciences
  • Online:2014-10-10 Published:2014-10-09

摘要: 西藏盐湖中碳酸盐型盐湖分布广泛,在蒸发过程中形成的含钾矿物以钾芒硝与氯化钾为主。以碱性碳酸盐型盐湖为研究对象,开发新捕收剂,利用浮选工艺从不同的含钾原矿中,浮选加工出品位较高的钾芒硝和氯化钾。在研究了解离度、捕收剂添加量、固液比、浮选时间、转速、充气量、精选实验等条件实验的基础上,确立了最佳闭路循环流程工艺条件。通过闭路循环实验,计算循环物料量,获得产品品位、钾离子收率等参数。实验表明,浮选工艺加工钾芒硝为主的矿物体系,钾元素收率高达98%,得到钾芒硝质量分数为91%以上的矿物。

关键词: 钾芒硝, 浮选工艺, 碳酸盐型盐湖

Abstract: The carbonate-based salt lakes are widely distributed in Tibet,China.Potassium minerals which were formed during the process of evaporation,were primarily glaserite and potassium chloride.To study alkaline carbonate salt lakes and to exploit new collectors,the flotation method was used to prepare higher grade glaserite and potassium chloride from different potassium ores.On the basis of the study on the degree of dissociation,collector dosage,solid-liquid ratio,flotation time,rotate speed,inflatable volume,and choiceness conditions etc.,the optimum process conditions of closed-loop process were established.Through closed-loop experiments,the amount of recyclable mineral,product grade,and yield coefficient of potassium ions etc.were calculated.Experimental results showed that in the glaserite-based mineral flotation system,the potassium yield reached 98% and the mass fraction of glaserite was above 91%.

Key words: glaserite, flotation process, carbonate-based salt lakes