无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2012, Vol. 44 ›› Issue (7): 22-.

• 论文 • 上一篇    下一篇

载银蛭石抗菌剂的制备及抗菌性能研究

孟桂花,吴建宁,但建明,杨 君,马存花,王国卫   

  1. 石河子大学化学化工学院,新疆兵团化工绿色过程重点实验室,省部共建国家重点实验室培育基地,新疆石河子 832003
  • 发布日期:2012-07-11

Study on preparation of silver loaded vermiculite and its antibacterial property

MENG  Gui-Hua, WU  Jian-Ning, DAN  Jian-Ming, YANG   Jun, MA  Cun-Hua, WANG  Guo-Wei-   

  1. Key Laboratory for Green Process of Chemical Engineering of Xinjiang Bingtuan,Ministry-province Jointly-constructed Cultivation
    Base for State Key Laboratory,School of Chemistry and Chemical Engineering,Shihezi University,Shihezi 832003,China
  • Published:2012-07-11

摘要: 以新疆伊犁蛭石为原料,首先对蛭石进行预处理,主要经过酸化、热处理及钠化处理,其次采用离子交换法制备了载银蛭石抗菌剂,最后通过对反应温度、反应时间、硝酸银浓度和pH对产品载银量影响的探讨,优化出制备载银蛭石的最佳工艺条件:反应温度为50 ℃;反应时间为5 h;硝酸银浓度为0.1 mol/L;pH为5。在最佳工艺条件下得到的产品载银量最大,最大载银量为5.23%(载银质量分数)。通过抑菌环法测试产品对大肠杆菌和金黄色葡萄球菌的抗菌活性,表明载银蛭石具有很强的抗菌性能。

关键词: 蛭石, 载银量, 离子交换法, 抗菌性

Abstract: Antibacterial agent silver loaded vermiculite was prepared by ion exchange method with vermiculite from Yili, Xinjiang Autonomous Region as raw material. During the preparation,vermiculite must be pre-treated at first,which mainly included acidification,heating treatment,and sodium treatment.Effects of reaction temperature,reaction time,silver nitrate concentration,and solution pH on amount of loaded silver were discussed.Results showed that the optimal reaction conditions were as follows:reaction temperature was 50 ℃,reaction time was 5 h,silver nitrate concentration was 0.1 mol/L,and pH=5.Under such conditions,the reaction product loaded the largest amount of silver and the maximum load was 5.23%.The antibacterial activity was tested for E.coli and Staphylococcus aureus by inhibition zone method,and results showed loaded silver vermiculite had strong antibacterial property.

Key words: vermiculite, amount of loaded silver, ion exchange, antibacterial property

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