无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2012, Vol. 44 ›› Issue (3): 36-.

• 论文 • 上一篇    下一篇

芒硝法生产硫酸钾水平衡问题讨论

张玉翠   

  1. 运城盐化设计院,山西运城044000
  • 发布日期:2012-03-12

Discussion on water balance for production of potassium sulfate by Glauber′s salt method

 ZHANG  Yu-Cui   

  1. Yuncheng Design Institute of Chemical Salt Industry,Yuncheng 044000,China
  • Published:2012-03-12

摘要: 芒硝法生产硫酸钾是利用两段转化、一次蒸发来完成硫酸钾及副产品工业盐的生产,整个系统封闭循环。在实际生产中,进入系统的水和流出系统的水达到平衡时整个系统才能稳定运行,但是二者受产品质量的制约很难达到平衡。对水不平衡问题进行了理论分析。详细论述了水不平衡对产品质量和整个系统的影响。找出了产生水不平衡的原因,并提出解决办法,即可通过调整一转化配料点提高钾芒硝质量、加开真空结晶器和强化蒸发提高残液质量、掌握工艺水和非工艺水的加入等一系列措施,解决系统的水不平衡问题。

关键词: 硫酸钾, 芒硝法, 水平衡

Abstract: Twice-conversion and once-evaporation are used during the production process of potassium sulfate and its by-product industrial salts by Glauber′s salt method,which is closed in a loop system.In the practical production,the whole system cannot reach the steady-state until the inflow and outflow of the water from the system get the balance.But it is hard to reach the balance due to the restriction of the product quality.In order to find out the cause and effect of the water imbalance and its corresponding solution,the effect of water imbalance on production quality and whole system was discussed on the basis of the theoretical analysis.That is,the water imbalance was expected to be solved through the following aspects, such as the adjustment of the conversion batching to improve the quality of potassium Glauber′s salt, the addition of vacuum crystallizer,the enhancement of evaporation to improve the quality of residue,the control of the addition of the process and non-process waters etc..

Key words: potassium sulfate;Glauber&prime, s salt method;water balance

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