Inorganic Chemicals Industry >
Determination of major component in inorganic coated titanium pigment by X-ray fluorescence spectrometry with pressed powder
Received date: 2020-08-10
Online published: 2021-05-12
A method of determination of TiO2 in inorganic coated titanium pigment by X-ray fluorescence spectrometry based on powder pressed sampling was established.A set of industrial inorganic coated titanium pigment were selected as the stan-dard samples and the content of the standard sample was analyzed by chemical titration as the standard sample value.The matrix effect was corrected by methods of empirical α coefficient and Compton scattering internal standard.A analytical curve was established and the measuring conditions and analytical methods were studied.The precision and accuracy experiments showed that the relative standard deviation（RSD） was 0.14% and the accuracy was reliable.
Wen Chen , Xiang Long , Yaqiu Jin , Duan Mao . Determination of major component in inorganic coated titanium pigment by X-ray fluorescence spectrometry with pressed powder[J]. Inorganic Chemicals Industry, 2021 , 53(5) : 93 -95 . DOI: 10.11962/1006-4990.2020-0343
| [1] | 龙翔, 胡劲, 刘建良, 等. 酸碱度对钛白粉铝包膜产品吸油量影响[J]. 云南冶金, 2016,45(3):74-77. |
| [2] | GB/T 1706—2006 二氧化钛颜料[S]. |
| [3] | 寸凤妹, 李小莉. X射线荧光光谱法测定钛白粉样品中10种微量元素[J]. 现代仪器与医疗, 2013,19(6):63-65. |
| [4] | 张建波, 朱丽辉, 林力. X-射线荧光光谱法测定钛白粉中磷铁锆铌[J]. 冶金分析, 2009,29(1):40-43. |
| [5] | 唐佳瑜. X射线荧光光谱法测定钛白粉中特定氧化物的含量[J]. 冶金管理, 2019(9):67,80. |
| [6] | 李化全, 郭传华. X-射线荧光光谱法测定二氧化钛微量元素标样的制备与探讨[J]. 涂料工业, 2013,43(2):56-58. |
| [7] | 王斌, 张江锋, 蒋小良, 等. X射线荧光光谱法测定皮革及其制品中的铅[J]. 理化检验:化学分册, 2015,51(6):869-871. |
| [8] | 钟坚海. 熔融制样-X射线荧光光谱法测定铝矿中15种组分[J]. 冶金分析, 2018,38(11):24-29. |
| [9] | 黄燕华, 张娜, 刘丽. X射线荧光光谱法测定海砂中TiO2和ZrO2含量[J]. 化工设计通讯, 2017,43(11):216-217. |
| [10] | 戴丽明, 耿晓红, 刘静, 等. ICP-AES法测定伪劣钛白粉中钙镁钡硅铝锌[J]. 无机盐工业, 2015,47(12):63-66. |
| [11] | 任玲玲. 电感耦合等离子体原子发射光谱法测定钛白粉中的微量元素[J]. 理化检验 :化学分册, 2017,53(7), 796-799. |
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