不同形貌纳米氧化铁的制备及性能研究

doi:10.11962/1006-4990.2018-0596

Abstract

Abstract:

The α-Fe₂O₃ were prepared by hydrothermal method,in which ferric nitrate hexahydrate as iron source,water and N,N-dimethylformamide（DMF） as solvents,and cetyldimethy-lammonium bromide（CTAB） and sodium dodecyl benzene sulfonate（SDBS） as surfactants,respectively.The as-prepared products were characterized and analyzed by X-ray diffraction （XRD）,fluorescent spectrometry（PL） and scanning electron microscope（SEM）.Results showed that the iron oxide nano- materials had different sizes and different morphologies under the action of different solvents and surfactants.The intensity of the photoluminescence emission peak was different,and the position of the emission peak was obviously red-shifted and blue-shifted,which were mainly attributed to the different sizes and different morphologies of the iron oxide nanomaterials.

Key words: α-Fe₂O₃, hydrothermal method, N,N-dimethylformamide, CTAB, SDBS

CLC Number:

TQ138.11

Wang Donghua,Fu Xin. Preparation and properties of iron oxide nanomaterials with different morphologies[J]. Inorganic Chemicals Industry, 2019, 51(9): 21-23.

Figures/Tables 4

References 15

[1]	赖雅文 . 纳米氧化铁的制备方法及其在涂料中的应用探讨[J]. 中国涂料, 2017,32(3):72-76.
[2]	鲁秀国, 黄林长, 杨凌焱 , 等. 纳米氧化铁制备方法的研究进展[J]. 应用化工, 2017,46(4):741-743.
[3]	伍媛婷, 王秀峰, 李二元 , 等. 纳米氧化铁粉体的溶胶-凝胶法制备[J]. 压电与声光, 2010,32(5):827-829.
[4]	徐锁平, 朱广军 . 超声波-均匀沉淀法制备纳米氧化铁[J]. 涂料工业, 2005,35(2):31-33.
[5]	Xiao L, Schroeder M, Kluge S , et al. Direct self-assembly of Fe₂O₃/reduced graphene oxide nanocomposite for high-performance lithi-um-ion batteries[J]. Journal of Materials Chemistry A, 2015,3(21):11566-11574.
[6]	翟明明, 杨继庆, 李维娜 , 等. 三种纳米Fe₂O₃的制备方法研究[J]. 中国医学物理学杂志, 2013,30(1):3936-3938.
[7]	李杰, 李焕莲 . α-Fe₂O₃纳米材料的合成及其在光催化中的应用[J]. 景德镇学院学报, 2015,30(6):29-31.
[8]	杜庆波 . 氧化铁纳米材料的制备、表征及磁性研究[J]. 硅酸盐通报, 2016,35(9):2922-2924.
[9]	陆希峰, 朱玲玲, 满杰 , 等. α-氧化铁纳米花的合成、表征与气敏性能研究[J]. 无机盐工业, 2017,49(9):35-37.
[10]	Hao S L, Wang X, Cui Y F , et al. Investigation on the agglomerate mechanism and controlling method in nano-particle powder preparation[J]. Journal of Synthetic Crystals, 2006,35(2):342-346.
[11]	魏玮 . 3H-1,2-二氢-1-吡咯里嗪酮衍生物的合成[D]. 天津:天津科技大学, 2009.
[12]	贺翠翠, 赵宁宁, 刘健冰 , 等. 纳米氧化铁的合成及对NTO热分解性能的影响[J]. 火炸药学报, 2013,36(5):29-34.
[13]	王天顺, 董晟全, 梁艳峰 , 等. 超声化学法制备纳米氧化铁粉体[J]. 化工新型材料, 2013,41(1):34-36.
[14]	Yang S K, Kiraly B, Wang W Y , et al. Fabrication and characteriza- tion of beaded SiC quantum rings with anomalous red spectral shift[J]. Advanced Materials, 2012,24(41):5598-5603.
[15]	Li H J, He Z B, Chu Y H , et al. Large-scale synjournal,growth mech-anism,and photoluminescence of 3C-SiC nanobelts[J]. Materials Letters, 2013,109(1):275-278.

样品编号	原料	表面活性剂	溶剂
1	九水合硝酸铁	CTAB	DMF
2	九水合硝酸铁	CTAB	水
3	九水合硝酸铁	SDBS	水
4	九水合硝酸铁	SDBS	DMF

National Inorganic Salts Information Center

Inorganic Acid-Base-Salt Committee of CIESC

Preparation and properties of iron oxide nanomaterials with different morphologies

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

Figures/Tables 4

References 15

Related Articles 15

Metrics

Comments

Recommended 10

[1]	Li Xiangguo,Guo Miao,Yao Huimin,Lü Jing. Research on hydrothermal synthesis and photoluminescence mechanism of rhombus CeO₂ [J]. Inorganic Chemicals Industry, 2020, 52(6): 30-35.
[2]	Guo Ju,Jia Shuangzhu. Study on the one-step hydrothermal synthesis of LiFePO₄ and its properties [J]. Inorganic Chemicals Industry, 2020, 52(6): 36-40.
[3]	Liu Ying. Synthesis of magnesium ferrite photocatalyst and degradation activity of various dyes [J]. Inorganic Chemicals Industry, 2020, 52(11): 103-107.
[4]	Huang Zhenxu,He Huanhuan,Jia Panpan,Chen Tiwei,Wei Shiqian. Synthesis of graphene by hydrothermal method and its electrocatalytic property on ascorbic acid [J]. Inorganic Chemicals Industry, 2020, 52(11): 29-32.
[5]	Chen Ping,Tian Yu,Hu Cheng. Effect of type and concentration of salt solution on synthesis of α-semi-water desulfurization gypsum [J]. Inorganic Chemicals Industry, 2020, 52(10): 130-134.
[6]	Wu Ruifeng1，Wang Hongwei2，Pi Xiaoyuan1. Study on MoS2 composite conductive carbon as anode material forhigh performance sodium ion battery [J]. Inorganic Chemicals Industry, 2019, 51(7): 28-32.
[7]	Zheng Shaocong1，Zhu Liping1，Xie Gang2，Wen Zhengjiao1. Experimental study on preparation of calcium sulfate whiskers from highpurity natural gypsum with hydrothermal method [J]. Inorganic Chemicals Industry, 2019, 51(7): 39-42.
[8]	Zhao Yu,Zhang Shuojia,Xu Bing,Yu Yue,Sun Xiaohui. Fabrication and electrochemical properties of Zn-based electrode materials [J]. Inorganic Chemicals Industry, 2019, 51(6): 21-24.
[9]	Lü Pin,Shi Chunhui,Li Wei,Zhong Jianchu. Controllable synthesis and characterization of thermal stabilizer Mg-Al-LDHs [J]. Inorganic Chemicals Industry, 2019, 51(6): 29-33.
[10]	Mao Qiqi,Liu Chuanxin,Dong Wenjuan,Zhang Ximan,Chen Hongyu,Wu Suwen. Preparation and characterization of spheniscidite [J]. Inorganic Chemicals Industry, 2019, 51(5): 53-56.
[11]	Xie Juan,Xia Runnan,Du Hongxia,Xu Yongquan,Zhao Shuchun,Xu Hong,Kang Wentong. Preparation of α-Fe₂O₃/coal gangue composite photocatalyst and its application in pentachlorophenol degradation [J]. Inorganic Chemicals Industry, 2019, 51(5): 74-77.
[12]	Li Xin1，Yuan Bo2，Yi Meigui1. Study on removal of trace sulfur impurities from lithium carbonate by hydrothermal method [J]. Inorganic Chemicals Industry, 2019, 51(11): 28-30.
[13]	TIAN Xi-Qiang, ZHAO Dong-Jiang, MA Song-Yan, CHI Cai-Xia, DONG Yan-Ping, TIAN Jun, QIAO Xiu-Li. Electrocatalytic performances of NiCo₂S₄ compound towards oxygen reduction [J]. INORGANICCHEMICALSINDUSTRY, 2016, 48(8): 74-.
[14]	LI Xiao-Yun, YU Hai-Bin, SUN Yan-Min, LI Shi-Peng, ZENG Xian-Jun, SUI Yun-Le, ZHOU Peng. Inorganic aluminum salt assisted hydrothermal synthesis of pseudoboehmite by activated alumina [J]. INORGANICCHEMICALSINDUSTRY, 2016, 48(6): 35-.
[15]	XU Xue-Tang, SU Hai-Yan, YU Liu-Hui, LIANG Yan-Yan, CHEN Kun, WANG Fan. Preparation and photocatalytic properties of Eu-doped BiVO4 micro-nano material [J]. INORGANICCHEMICALSINDUSTRY, 2016, 48(5): 61-.