Research & Development

Study on application of Raman mapping technology in characterization of composition,defects and stress distribution of lithium tantalate crystal

  • Zhifeng Guo
Expand
  • CHN ENERGY Zhungeer Energy Co.,Ltd.,Erdos 010300,China

Received date: 2021-02-19

  Online published: 2021-10-11

Abstract

The Raman mapping test of lithium tantalate crystal was studied by laser raman microscopy spectrometer.The com-position distribution of lithium tantalate crystal was imaged by Raman mapping in the characteristic peak intensity of 865 cm-1.The Li content distribution of crystal was imaged by Raman mapping in the characteristic peak FWHM of 865 cm-1.The de-fects distribution of crystal was imaged by Raman mapping in the defects peak intensity of 750 cm-1.The stress distribution of crystal was imaged by Raman mapping in the characteristic peak position of 865 cm-1.The test results showed the composi-tion,defects and stress distribution of lithium tantalate single crystal sheet could be well imaged by Raman mapping.The composition and Li content distribution of undoped lithium tantalate crystal were more uniform than that doped with Fe2O3.The distribution of intrinsic defects in undoped and doped lithium tantalate crystals with Fe2O3 was both relatively uniform and few.The stress distribution of undoped lithium tantalate crystal was more uniform than that doped with Fe2O3.There was an obvious stress concentration region in lithium tantalate crystal doped with Fe2O3.

Cite this article

Zhifeng Guo . Study on application of Raman mapping technology in characterization of composition,defects and stress distribution of lithium tantalate crystal[J]. Inorganic Chemicals Industry, 2021 , 53(10) : 70 -73 . DOI: 10.19964/j.issn.1006-4990.2021-0102

References

[1] Juvalta F, Jazbinsek M, Gunter P. Electro-optical properties of near-stoichiometric and congruent lithium tantalite at ultraviolet wave-lengths[J]. J.Opt.Soc.Am.B, 2006, 23:276-281.
[2] Xu P, Zhao L N, Lv X J, et al. Compact high-power red-green-blue laser light source generation from a single lithium tantalite with cascaded domain modulation[J]. Optics Express, 2009, 17:9509-9514.
[3] Imbrock J, Wevering S, Buse K. Nonvolatile holographic storage in photorefractive lithium tantalate crystals with laser pulses[J]. J.Opt.Soc.Am.B, 1999, 16:1392-1397.
[4] Lange K, Rapp B E, Rapp M. Surface acoustic wave biosensors:A review[J]. Anal.Bioanal.Chem., 2008, 391:1509-1519.
[5] Ganesamoorthy S, Nakamura M, Takekawa S, et al. A comparative study on the domain switching characteristics of near stoichiometric lithium niobate and lithium tantalate single crystals[J]. Materials Science and Engineering B, 2005, 120:125-129.
[6] Lines M E, Glass A M. Primary pyroelectric effect in LiTaO3[J]. Phys.Rev.Lett., 1977, 39:1362-1365.
[7] 吴娟霞, 徐华, 张锦. 拉曼光谱在石墨烯结构表征中的应用[J]. 化学学报, 2014(3):301-318.
[8] 杨昕梅, 孙泽, 黄龙, 等. 相变储能二元混合硝酸盐的Raman光谱研究[J]. 无机盐工业, 2016, 48(2):18-21.
[9] 张福生, 陈秀芳, 崔潆心, 等. Ge掺杂碳化硅晶体的生长缺陷[J]. 无机材料学报, 2016(11):1166-1170.
[10] 李亚, 丁敏娟, 李蓉, 等. 黏土基二氧化钛水热制备及其光催化性能研究[J]. 无机盐工业, 2018, 50(12):75-78.
[11] 胡成龙, 陈韶云, 陈建, 等. 拉曼光谱技术在聚合物研究中的应用进展[J]. 高分子通报, 2014(3):30-45.
[12] 路交, 朱珊珊, 崔笑宇, 等. 拉曼光谱成像技术及其在生物医学中的应用[J]. 中国激光, 2018(3):70-79.
[13] 沈大娲, 郑菲, 吴娜, 等. 拉曼光谱在文物考古领域的应用态势分析[J]. 光谱学与光谱分析, 2018(9):2657-2664.
[14] 赵业权, 贾宝申, 张学锋, 等. 掺镁近化学计量比LiTaO3晶体生长及光学性能[J]. 硅酸盐学报, 2007, 36(8):995-997.
[15] 师丽红, 孔勇发, 阎文博, 等. 近化学计量比钽酸锂晶体的拉曼光谱研究[J]. 人工晶体学报, 2005(6):1024-1029.
[16] 袁方方, 葛培琪, 高玉飞. KDP晶体缺陷对生长应力分布的影响[J]. 人工晶体学报, 2011(6):1435-1439.
[17] 王邦国, 李明伟, 周川. 三维运动下KDP晶体生长过程中的应力分析[J]. 人工晶体学报, 2014(12):3098-3103.
[18] 邓亚, 张宇民, 周玉锋. 碳化硅单晶材料残余应力检测技术研究进展[J]. 材料导报, 2019(S2):206-209.
Outlines

/