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Preparation of PS/Ag-SiO2-Au organic-inorganic bimetallic hybrid particles
Received date: 2020-03-14
Online published: 2020-09-27
PS/SiO2-Au organic-inorganic hybrid particles were obtained by reacting organic polystyrene dimer(PsD) with inorganic SiO2-Au particles.The snowman-shape of PsD particles and SiO2-Au particles were obtained via seed emulsion polymerization and sol-gel method,respectively.On the basis of PS/SiO2-Au particles,nano-sized Ag particles were supported on it to obtain bimetallic hybrid particles PS/Ag-SiO2-Au.During the period,effects of the ratios between monomers and polymer seeds,the adding amount of ammonia on morphology of the organic and inorganic particles were discussed.Infrared(FT-IR),scanning electron microscopy(SEM),energy spectrum analysis(EDS),transmission electron microscopy(TEM)and laser particle size tester(DLS) were used to characterize the structure,morphology,composition and size of the obtained particles.The prepared PS/Ag-SiO2-Au hybrid particles will have potential applications in the field of catalysis.
Key words: polystyrene dimers; silica; hybrid particles
Shuxing Mei , Shuanlin Pang , Mingwang Pan , Zhiyong Xie , Zhishui Li . Preparation of PS/Ag-SiO2-Au organic-inorganic bimetallic hybrid particles[J]. Inorganic Chemicals Industry, 2020 , 52(9) : 26 -31 . DOI: 10.11962/1006-4990.2019-0523
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