INORGANICCHEMICALSINDUSTRY ›› 2010, Vol. 0 ›› Issue (11): 0-0.

   

Preparation of 13X zeolite granular absorbent and study on its effect of absorbing calcium ion

Zhao Qiwen,Zhang Xingru,Tu Lanying,Cui Xiaoqin   

  • Online:2010-11-10 Published:2010-10-01

Abstract: <SPAN lang=EN-US style="FONT-SIZE: 10.5pt; FONT-FAMILY: "Times New Roman"; mso-bidi-font-size: 12.0pt; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA; mso-fareast-font-family: 宋体">A granular absorbent was prepared by adding binder,pore-agent,water and so on to 13X zeolite powder,then it was obtained through drying,high temperature calcined molding,crushing,and screening.The granular absorbent could be used to absorp calcium ions in solution.Types of binder were screened and the influences of raw material ratio,calcination temperature,particle size,adsorption time etc.on the loss rate of granular adsorbent in water and on the absorption effect of calcium ions were studied.Results showed that the granular adsorbent had optimum performance when palygorskitet served as binder,the mass ratio of material 13X zeolite,clay,and fine coal powder was 15</SPAN><SPAN style="FONT-SIZE: 10.5pt; FONT-FAMILY: 宋体; mso-bidi-font-size: 12.0pt; mso-ascii-font-family: "Times New Roman"; mso-hansi-font-family: "Times New Roman"; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA">∶</SPAN><SPAN lang=EN-US style="FONT-SIZE: 10.5pt; FONT-FAMILY: "Times New Roman"; mso-bidi-font-size: 12.0pt; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA; mso-fareast-font-family: 宋体">4</SPAN><SPAN style="FONT-SIZE: 10.5pt; FONT-FAMILY: 宋体; mso-bidi-font-size: 12.0pt; mso-ascii-font-family: "Times New Roman"; mso-hansi-font-family: "Times New Roman"; mso-bidi-font-family: "Times New Roman"; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA">∶</SPAN><SPAN lang=EN-US style="FONT-SIZE: 10.5pt; FONT-FAMILY: "Times New Roman"; mso-bidi-font-size: 12.0pt; mso-font-kerning: 1.0pt; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA; mso-fareast-font-family: 宋体">1,and calcination temperature was <?xml:namespace prefix = st1 ns = "urn:schemas-microsoft-com:office:smarttags" /><st1:chmetcnv w:st="on" TCSC="0" NumberType="1" Negative="False" HasSpace="True" SourceValue="650" UnitName="℃">650 <SPAN lang=EN-US style="FONT-FAMILY: 宋体; mso-ascii-font-family: "Times New Roman"; mso-hansi-font-family: "Times New Roman""><SPAN lang=EN-US>℃</SPAN></SPAN></st1:chmetcnv>.Moreover,calcium absorption capacity was up to 25.31 mg/g,and the loss rate was only 1.98%.Decreased adsorbent particle size could significantly increase the adsorption rate,extended the absorption time made adsorption capacity rise,and adsorbed 120 min could reach basic saturation.Static isothermal adsorption process was in accord with Langmiur isotherm equation.</SPAN>