无机盐工业
主管:中海油天津化工研究设计院有限公司
主办:中海油天津化工研究设计院有限公司
   中海油炼油化工科学研究院(北京)有限公司
   中国化工学会无机酸碱盐专业委员会
ISSN 1006-4990 CN 12-1069/TQ

无机盐工业 ›› 2013, Vol. 45 ›› Issue (5): 35-.

• 论文 • 上一篇    下一篇

热溶冷结晶法制取硫酸钾镁肥的实验研究

谈 霞,李宏灿   

  1. 青海中信国安科技发展有限公司,青海格尔木  816000
  • 发布日期:2013-05-03

Study on preparation of potassium-magnesium sulfate fertilizer with thermally dissolved cold crystallization method

 TAN   Xia, LI  Hong-Can   

  1. Qinghai CITIC Guoan Technology Development Co.,Ltd.,Germu 816000,China
  • Online:2013-05-03

摘要: 采用西台吉乃尔盐湖卤水利用大盐田生产日晒得到的钾、硫混盐矿作为原料,通过热溶冷结晶工艺制取无药剂污染的硫酸钾镁肥。结果表明:热溶冷结晶法制取硫酸钾镁肥工艺可行,原矿硫钾质量比和原矿粒度、热溶过程中热溶温度和时间、冷结晶过程冷却时间和温度等因素是影响系统钾收率的主要条件,并通过不同原矿粒度、热溶溶剂及不同混合比例、转化液加入量、热溶温度、时间及冷结晶时间、温度等单因素实验得到最佳实验条件。

关键词: 硫酸钾镁肥, 热溶冷结晶, 钾硫混盐矿

Abstract: Potassium-magnesium sulfate fertilizer without pharmaceutical pollution was prepared by thermally dissolved cold crystallization technology with potassium-sulfate mixed salt mine from solar evaporation of sulfate-type West Taijinar salt lake brine as raw material. Results showed that the preparation technology of potassium-magnesium sulfate fertilizer with thermally dissolved cold crystallization method was feasible.The mass ratio of potassium to sulfate and granularity of the mine,thermally dissolved temperature and time,and cooling temperature and time were the main conditions affecting potassium yield.Optimum technological conditions of the preparation of potassium-magnesium sulfate fertilizer were obtained by single-factor experiments,such as different granularities,different thermally dissolved solvents and mixture ratios,reaction liquid quantities, and thermally dissolved temperatures and times etc..

Key words: potassium-magnesium sulfate fertilizer, thermally dissolved cold crystallization, potassium-sulfate mixed salt mine

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