INORGANICCHEMICALSINDUSTRY ›› 2010, Vol. 0 ›› Issue (6): 0-0.
Xu Dongmei,Tian Weiliang,Li Xinyu,Cong Minghui,Qi Wei,Xu Nuo
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Abstract: <FONT face=Verdana>A process route that reclaiming silicon carbide from drained slurry generated by cutting silicon crystal with wire-saw and simultaneously using its recovery solution to prepare white carbon black was introduced.Silicon carbide was reclaimedfirstly by high-concentration alkali-soluble method to dissolve silicon in drained slurry,and then white carbon black was prepared by hydrochloric acid replacing sulfuric acid and sodium chloride to promote salting-out and by n-butanol to control particle growth and agglomeration.Reaction between sodium hydroxide and silicon in drained slurry and acidizingreaction of water glass were studied.Results showed that the optimum conditions for the two reactions respectively were as follows:mass concentration of sodium hydroxide was 0.25~0.35 g/mL and temperature was about 55 ℃;mass fraction of sodium silicate was 9%~12%,mass fraction of hydrochloric acid was 20%~25%,n-butanol was 13 drops(approximately0.6 mL),and temperature was about 80 ℃.Technology realized the reasonable utilization of silicon in drained slurry. </FONT>
Xu Dongmei;Tian Weiliang;Li Xinyu;Cong Minghui;Qi Wei;Xu Nuo. Study on preparation technology of white carbon black from drained slurry generated by cutting silicon crystal with wire-saw[J]. INORGANICCHEMICALSINDUSTRY, 2010, 0(6): 0-0.
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