INORGANICCHEMICALSINDUSTRY ›› 2014, Vol. 46 ›› Issue (3): 19-.

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Process research on preparation of sodium silicate by purified diatomite

 HU  Zhi-Bo, LI  Jia-Wang, ZHENG  Shui-Lin, YAN   Yang, XU  Chun-Hong   

  1. School of Chemical & Environmental Engineering,China University of Mining and Technology,Beijing 100083,China
  • Online:2014-03-10 Published:2014-03-07

Abstract: The main chemical component of diatomite is amorphous silica.Preparation technology of sodium silicate by water-heated alkali reaction and with Linjiang low-grade diatomite after mineral processing was studied.The influences of the time and temperature of alkali-dissolved reaction,mass ratio of liquid to solid and mass ratio of sodium hydroxide to diatomite on the dissolution rate of silica as well as on Si/Na ratio of sodium silicate were investigated.Results showed that dissolution rate of SiO2 improved and the Si/Na ratio decreased obviously as the mass ratio of sodium hydroxide /diatomite increased under the same conditions.It was verified that the optimal experiment results:dissolution rate of SiO2 was 93.22%,Si/Na ratio of sodium silicate was 0.96,and the output ratio of sodium silicate was 169.35 g when diatomite was 100 g  under the conditions as following: time of alkali-dissolved reaction was 90 min,the temperature of alkali-dissolved reaction was 96 ℃,mass ratio of liquid to solid was 2.5,and mass ratio of sodium hydroxide /diatomite was 1.24. 

Key words: purified diatomite, water-heated alkaline reaction, sodium silicate

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